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Structural methods in molecular inorganic chemistry
Title statement Structural methods in molecular inorganic chemistry / David Rankin, Carole Morrison, Norbert Mitzel Personal name Rankin, David W. H. (author) Publication Chichester : Wiley, 2013 Phys.des. 1 online zdroj ISBN 9781118462881 (online) 1118462882 (online) 9780470975572 (Adobe PDF) 0470975571 (Adobe PDF) 9781118462904 (MobiPocket) 1118462904 (MobiPocket) 9781118462898 (online) 1118462890 (online) 0470972793 (Cloth) 9780470972793 (Cloth) 9781283949965 (MyiLibrary) 1283949962 (MyiLibrary) Edition Inorganic chemistry Internal Bibliographies/Indexes Note Obsahuje bibliografické odkazy a rejstřík Contents Structural Methods in Molecular Inorganic Chemistry; Contents; Preface; Companion Website; Acknowledgements; Biographies; 1. Determining Structures -- How and Why; 1.1 Structural chemistry -- where did it come from?; 1.2 Asking questions about structure; 1.3 Answering questions about structure; 1.4 Plan of the book; 1.5 Supplementary information; 2. Tools and Concepts; 2.1 Introduction; 2.2 How structural chemistry techniques work; 2.3 Symmetry; 2.3.1 Symmetry operations and elements; 2.3.2 Point groups; 2.3.3 Characters, character tables and symmetry species; 2.4 Electron density. Content note 2.5 Potential-energy surfaces2.6 Timescales; 2.7 Structural definitions; 2.8 Sample preparation; 2.8.1 Unstable species; 2.8.2 Solutions in supercritical fluids; 2.8.3 Involatile species; 2.8.4 Variable temperature and pressure measurements; 2.9 Quantitative measurements; 2.10 Instrumentation; 2.10.1 Radiation sources; 2.10.2 Detectors; 2.11 Data analysis; 2.11.1 Fourier transformation; 2.11.2 Experimental errors and uncertainties; 2.11.3 Least-squares refinement; 2.11.4 Database mining; Review questions; Discussion problems; References; 3. Theoretical Methods; 3.1 Introduction.. 3.8 Comparing theory with experiment: molecular properties3.8.1 Vibrational spectra; 3.8.2 NMR, EPR and Mössbauer spectra; 3.8.3 Molecular orbitals; 3.8.4 Electronic spectra; 3.8.5 Modeling solvent effects; 3.9 Combining theory and experiment; Review questions; Discussion problems; References; 4. Nuclear Magnetic Resonance Spectroscopy; 4.1 Introduction; 4.2 The nuclear magnetic resonance phenomenon; 4.3 Experimental set-up; 4.3.1 NMR spectrometers; 4.3.2 Sample preparation; 4.3.3 Continuous wave and Fourier transform spectra; 4.4 The pulse technique; 4.4.1 Inducing magnetization by a pulse.. 4.4.2 Relaxation of magnetization after a pulse4.4.3 Free induction decay and Fourier transformation; 4.5 Information from chemical shifts; 4.5.1 General principles; 4.5.2 Proton chemical shifts; 4.5.3 Chemical shifts of other elements; 4.6 Information from NMR signal intensities; 4.7 Simple splitting patterns due to coupling between nuclear spins; 4.7.1 First-order spectra of spin-1/2 isotopes of 100% abundance; 4.7.2 Nuclear spin systems; 4.7.3 Coupling to spin-1/2 isotopes of low abundance; 4.7.4 Spectra of spin-1/2 isotopes of low abundance; 4.7.5 Coupling to quadrupolar nuclei. Notes to Availability Přístup pouze pro oprávněné uživatele Note Způsob přístupu: World Wide Web Defekty eBooks on EBSCOhost Another responsib. Morrison, Carole A., 1972- (author) Mitzel, Norbert W., 1966- (author) Tištěná verze knihy Subj. Headings struktura molekul molecular structure * anorganická chemie inorganic chemistry Form, Genre elektronické knihy electronic books Conspect 546 - Anorganická chemie UDC 544.112.022-122 , 546 , (0.034.2:08) Country Anglie Language angličtina Document kind Electronic sources URL http://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&AN=522920 book
"Structural Methods in Molecular Inorganic Chemistry is designed to help readers interpret experimental data, understand the material published in modern journals of inorganic chemistry, and make decisions about what techniques will be the most useful in solving particular structural problems"--
Structural Methods in Molecular Inorganic Chemistry; Contents; Preface; Companion Website; Acknowledgements; Biographies; 1. Determining Structures -- How and Why; 1.1 Structural chemistry -- where did it come from?; 1.2 Asking questions about structure; 1.3 Answering questions about structure; 1.4 Plan of the book; 1.5 Supplementary information; 2. Tools and Concepts; 2.1 Introduction; 2.2 How structural chemistry techniques work; 2.3 Symmetry; 2.3.1 Symmetry operations and elements; 2.3.2 Point groups; 2.3.3 Characters, character tables and symmetry species; 2.4 Electron density.2.5 Potential-energy surfaces2.6 Timescales; 2.7 Structural definitions; 2.8 Sample preparation; 2.8.1 Unstable species; 2.8.2 Solutions in supercritical fluids; 2.8.3 Involatile species; 2.8.4 Variable temperature and pressure measurements; 2.9 Quantitative measurements; 2.10 Instrumentation; 2.10.1 Radiation sources; 2.10.2 Detectors; 2.11 Data analysis; 2.11.1 Fourier transformation; 2.11.2 Experimental errors and uncertainties; 2.11.3 Least-squares refinement; 2.11.4 Database mining; Review questions; Discussion problems; References; 3. Theoretical Methods; 3.1 Introduction.3.8 Comparing theory with experiment: molecular properties3.8.1 Vibrational spectra; 3.8.2 NMR, EPR and Mössbauer spectra; 3.8.3 Molecular orbitals; 3.8.4 Electronic spectra; 3.8.5 Modeling solvent effects; 3.9 Combining theory and experiment; Review questions; Discussion problems; References; 4. Nuclear Magnetic Resonance Spectroscopy; 4.1 Introduction; 4.2 The nuclear magnetic resonance phenomenon; 4.3 Experimental set-up; 4.3.1 NMR spectrometers; 4.3.2 Sample preparation; 4.3.3 Continuous wave and Fourier transform spectra; 4.4 The pulse technique; 4.4.1 Inducing magnetization by a pulse.4.4.2 Relaxation of magnetization after a pulse4.4.3 Free induction decay and Fourier transformation; 4.5 Information from chemical shifts; 4.5.1 General principles; 4.5.2 Proton chemical shifts; 4.5.3 Chemical shifts of other elements; 4.6 Information from NMR signal intensities; 4.7 Simple splitting patterns due to coupling between nuclear spins; 4.7.1 First-order spectra of spin-1/2 isotopes of 100% abundance; 4.7.2 Nuclear spin systems; 4.7.3 Coupling to spin-1/2 isotopes of low abundance; 4.7.4 Spectra of spin-1/2 isotopes of low abundance; 4.7.5 Coupling to quadrupolar nuclei.
Number of the records: 1